Investigating different physical and/or chemical forms of...

G - Physics – 01 – N

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G01N 35/02 (2006.01) B01J 19/00 (2006.01) B01L 3/00 (2006.01) C07B 61/00 (2006.01)

Patent

CA 2372416

Apparatus and a method are described for investigating polymorphs of a material, isomers of a material which allow different isomeric forms to be resolved, different hydrates/solvates and/or different salts of a material. The apparatus comprises an assembly (2) of reactor devices (6) arranged within a reactor body (8) which incorporates a heating/cooling block (10) and a stirrer block (12). A vessel support block (14) supports respective sample vessels (15) below each reactor device (6) for receiving material from the reactor devices. The apparatus includes a control unit (4) which includes a computer (16) which controls a robot for delivering materials to the reactor devices; a heating/cooling unit (18); a stirrer control unit (20); and a pressure unit (22) which controls the passage of material from the reactor devices (6) to the sample vessels (15).

L'invention porte sur un appareil et des procédés de recherche de polymorphes et d'isomères dans un matériau qui permettent la dissolution des différentes formes isomères, des différents hydrates/solvates et/ou des différents sels d'un matériau. Cet appareil comprend un ensemble (2) de réacteurs (6) disposés dans un corps (8) qui renferme une unité de chauffage/refroidissement (10) et un agitateur (12). Une unité de support (14) supporte des réceptacles (15) d'échantillons placés au-dessous de chaque réacteur (6) de façon à recevoir le matériau des réacteurs. L'appareil comprend également une unité de commande (4) incluant un ordinateur (16) qui commande un robot distribuant les matériaux aux réacteurs ; une unité de chauffage/refroidissement (18); une unité de commande (20) d'agitateur et une unité de pression (22) qui commande le passage du matériau des réacteurs (6) aux réceptacles (15) d'échantillons.

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