Lewis base complexes of alkali metal salts

Details Lewis base complexes of alkali metal salts Lewis base complexes of alkali metal salts

C - Chemistry, Metallurgy

07

F

260/361, 260/438

C07F 1/00 (2006.01) C07F 9/22 (2006.01) C07F 9/24 (2006.01)

Patent

CA 1336000

Disclosed is a process for the manufacture of alkali metal salt complexes of the formula (MxX. nL)y, where M is an alkali metal e.g. lithium, X is an anion, e.g. halide or thiocyanate, L is an organic electron-donating ligand (Lewis base, x is the valency of the anion X, n is usually 1, 2 or 4 and y is integer, by the in situ reaction of an alkali metal or an alkali metal hydride or alkyl, for example lithium, lithium hydride or butyl lithium, and an anhydrous ammonium salt comprising the anion X, e.g. an anhydrous ammonium halide, the reaction being performed in solution in an anhydrous solvent in the presence of the ligand (L).

580823

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