Liposome preparation and material encapsulation method

A - Human Necessities – 61 – K

Patent

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A61K 9/127 (2006.01)

Patent

CA 2153251

The present invention relates to a method of producing liposomes useful for encapsulating and delivering a wide variety of biologically active materials. The invention provides liposomes and a production method which is simple, feasible and inexpensive for the large-scale commercial manufacturing of liposomes and encapsulated materials. The method involves the formation of a liposome dispersion in the absence of an organic solvent or detergent, one or several cycles of freezing and thawing the liposomes, and dehydration of the liposome dispersion to form a lipid powder. When desired, the lipid powder is hydrated in the presence of the biologically active material whereby the material is encapsulated in reconstituted liposomes. The method can also include combining the liposome dispersion with a bulking agent prior to the dehydration and formation of the lipid powder. The addition of the bulking agent facilitates the handling of the lipid powder as well as its rapid dispersal upon hydration.

La présente invention se rapporte à un procédé de production de liposomes utiles pour encapsuler et administrer une grande variété de matières biologiquement actives. L'invention concerne des liposomes et un procédé de production qui est simple, réalisable et peu coûteux pour une fabrication sur grand échelle de liposomes et de matières encapsulées. Ce procédé consiste à former une dispersion de liposomes en l'absence d'un solvant ou détergent organique, à générer un ou plusieurs cycles de congélation et décongélation des liposomes, et à déshydrater la dispersion de liposomes afin d'obtenir une poudre lipidique. Si on le souhaite, la poudre lipidique peut être déshydratée en présence d'une matière biologiquement active, cette matière étant encapsulée dans des liposomes reconstitués. Ce procédé peut également consister à combiner la dispersion de liposomes avec un diluant avant la déshydration et la formation de la poudre lipidique. L'addition d'un diluant facilite la manipulation de la poudre lipidique ainsi que sa dispersion rapide lors de l'hydratation.

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