Liquid-liquid extraction device and on-line transfer to a...

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G01N 30/04 (2006.01) G01N 30/18 (2006.01) G01N 30/24 (2006.01) G01N 30/06 (2006.01) G01N 30/14 (2006.01)

Patent

CA 2389042

An extraction device for liquid-liquid extraction of at least one analyte from a sample and on-line transfer of said analyte(s) to a gas chromatography apparatus is described, wherein said extraction device comprising a membrane- based extraction unit (1), a sample inlet (2), a sample outlet (3), and an organic liquid inlet (5), wherein it also comprises a needle (4) to be connected with a gas chromatography apparatus injector for the on-line transfer of the analyte(s) from the membrane-based extraction unit (1) to the gas chromatography apparatus via the needle (4), an organic liquid being immobilised as a stagnant phase in a volume of less than of less than 20 µl in the membrane-based extraction unit (1).

L'invention concerne un dispositif d'extraction liquide-liquide permettant d'extraire au moins une substance à analyser d'un échantillon et de transférer en direct la ou les substance(s) à analyser à un appareil de chromatographie en phase gazeuse. Ce dispositif d'extraction comprend une unité d'extraction à membrane (1), une entrée d'échantillon (2), une sortie d'échantillon (3) et une entrée de liquide organique (5). Ce dispositif comprend également une aiguille (4) destinée à être raccordée à l'injecteur d'un appareil de chromatographie en phase gazeuse pour le transfert en direct de la ou des substance(s) à analyser depuis l'unité d'extraction à membrane (1) jusqu'à l'appareil de chromatographie en phase gazeuse via l'aiguille (4). Un liquide organique est immobilisé comme phase stagnante dans un volume inférieur à 20 µl dans l'unité d'extraction à membrane (1).

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