Liquid-phase electrochemical reaction with particulate...

Details Liquid-phase electrochemical reaction with particulate... Liquid-phase electrochemical reaction with particulate...

C - Chemistry, Metallurgy

25

B

204/43.5

C25B 3/02 (2006.01) C25B 1/00 (2006.01) C25B 3/00 (2006.01) C25B 15/00 (2006.01)

Patent

CA 1149325

- 9 - ABSTRACT ELECTROCHEMICAL SYNTHESIS AND PRODUCT A liquid-phase electrochemical synthesis is possible wherein a desired charged intermediate would normally be undesirably immediately electrolysed, by covalently trapping the charged-intermediate onto particles of a sulphonated poly- styrene, filtering off the liquid, and regenerating the poly- styrene in (say) alkali to release and hydrolyse the intermediate. Hexamethylbenzene may be electrolysed in acetonitrile to give, by this process, 1, 3-(2, 4, 5, 6-tetramethyl)-bisacetamido- methylbenzene.

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