C - Chemistry – Metallurgy – 04 – B
Patent
C - Chemistry, Metallurgy
04
B
25/134, 319/60
C04B 35/10 (2006.01) B28B 3/02 (2006.01) C04B 35/113 (2006.01) C04B 37/00 (2006.01) H01M 2/16 (2006.01) H01M 10/39 (2006.01)
Patent
CA 1314929
ABSTRACT OF THE DISCLOSURE The invention provides a method of making a composite beta-alumina artifact, such as a separator tube for an electochemical cell, comprising two beta-alumina portions which are sealed together in a sealing zone, namely an inner portion and an outer portion which extends peripherally around the inner portion and embraces it in the sealing zone. The method comprises pressing the inner and outer portions from powders which, when sintered, shrink and form integral beta-alumina artifacts. The portions are then arranged so that the outer portion extends around the inner portion and embraces it in a sealing zone. The portions are then sintered to cause them to seal together hermetically in the sealing zone while converting each of the portions into a beta-alumina artifact. The portions are made so that the outer portion undergoes a greater degree of shrinkage during sintering than the inner portion and the portions are pressed so that the spacing between the portions where the outer portion extends around and embraces the inner portion is such that, upon sintering, the outer portion shrinks on to the inner portion to provide a hermetic peripheral seal between the portions.
579326
Duncan James Hugh
Stead Rodney James
Lilliwyte Societe Anonyme
Sim & Mcburney
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