Manufacture of solid ammonium phosphate

C - Chemistry – Metallurgy – 01 – B

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C01B 25/28 (2006.01) C05B 7/00 (2006.01)

Patent

CA 1052978

ABSTRACT OF THE DISCLOSURE The invention relates to a process for the manufacture of solid monammonium phosphate with good granulation properties suitable for use in compound fertiliser manufacture. An improvement in product quality is obtained when between 20% and 80% of an aqueous slurry of ammonium phosphate, formed by the ammoniation of wet-process phosphoric acid, is mixed with a second acid prior to entry into a moisture disengagement unit. This treatment precipitates some monammonium phosphate crystals which provide nuclei for further crystal growth. After a short time delay to allow crystals to form, the remainder of the slurry is then added separately to the moisture disengagement unit.

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