Manufacture of sulfenamides

Details Manufacture of sulfenamides Manufacture of sulfenamides

C - Chemistry, Metallurgy

07

D

260/309.3, 260/2

C07D 417/12 (2006.01) C07D 277/80 (2006.01)

Patent

CA 1145335

ABSTRACT OF THE DISCLOSURE A process for the manufacture of sulfenamides by the oxidation of a mixture of 2-mercaptobenzothiazole and the appropriate amine in a critical amount of water and/or organic solvent produces a pure product of good quality and high yield. The amount of water should be in the range of from 10 to 30% by weight based on the total reaction mixture.

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