C - Chemistry – Metallurgy – 07 – C
Patent
C - Chemistry, Metallurgy
07
C
C07C 249/02 (2006.01) C07C 251/24 (2006.01) C07D 207/448 (2006.01) C07D 209/48 (2006.01) C07D 209/66 (2006.01) C07D 221/14 (2006.01) C07D 251/70 (2006.01)
Patent
CA 2668464
The subject invention pertains to methods for solid-state synthesis of imides and imines using co-crystals. The co-crystal formers utilized are substrates of condensation reactions and co-crystals can be obtained in high yield via methods such as slurrying, solvent evaporation, solvent crystallization, treatment with supercritical fluid(s), melting plus crystallization, slurry conversion, grinding of solids, blending of powders, heating of solids, solvent-drop grinding, or grinding plus melting.
L'invention concerne des procédés de synthèse en phase solide d'imides et d'imines au moyen de co-cristaux. Les formeurs de co-cristaux utilisés sont des substrats de réactions de condensation et les co-cristaux peuvent être obtenus à haut rendement par la mise en AEuvre de procédés tels que la mise en suspension, l'évaporation de solvant, la cristallisation de solvant, le traitement par fluide(s) supercritique(s), la fusion plus cristallisation, la conversion de suspension épaisse, le broyage de matières solides, le mélange de poudres, le chauffage de matières solides, le broyage par gouttes de solvant ou le broyage plus fusion.
Cheney Miranda L.
Zaworotko Michael J.
Smart & Biggar
University Of South Florida
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