Method and apparatus for making novel particulate compositions

G - Physics – 01 – N

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150/11, 167/114,

G01N 33/96 (2006.01) A01N 1/02 (2006.01) A61K 9/19 (2006.01) A61K 35/16 (2006.01) A61K 38/00 (2006.01) C12N 1/04 (2006.01) C12N 9/98 (2006.01) F25C 1/00 (2006.01) F25D 3/10 (2006.01) F26B 5/06 (2006.01) G01N 33/483 (2006.01)

Patent

CA 1119953

ABSTRACT OF THE DISCLOSURE An improved method and apparatus is disclosed for producing frozen particulate compositions from liquid feed- stock. A continuous stream of liquid feedstock is passed through an orifice and into a liquid freezant without the orifice contacting the freezant. Compositions produced by this improved method have low proportions of fine and large particles, yielding particularly beneficial resulting in the case of quality control materials. The compositions are advantageously employed in automated weighing and filling apparatus.

318401

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