Method and apparatus for modulated differential analysis

G - Physics – 01 – N

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G01N 25/20 (2006.01) G01N 25/18 (2006.01) G01N 25/48 (2006.01)

Patent

CA 2089225

The present invention relates to differential analytical techniques for determining the composition, phase, structure, identification or other properties of a material that undergoes a transition as function of a driving variable. As applied to differential scanning calorimetric analysis (DSC), the preferred embodiment comprises: (1) heating a sample of the material with a linear temperature ramp that is modulated with a sinusoidal heating rate oscillation; and (2) deconvoluting the resultant heat flow signal into rapidly reversible and non-rapidly reversible components.

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