Method and device for producing nickel sulphamate

C - Chemistry – Metallurgy – 01 – B

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C01B 21/096 (2006.01)

Patent

CA 2426749

The method allows for nickel sulphamate to be produced by means of reacting elementary nickel with sulphamic acid. Therein, the nickel is disintegrated by strong stirring, mixing, or dispersing of the nickel-acid mixture by means of a stirring, mixing, or dispersing tool, introducing high energy density into the reaction mixture. Herein, the nickel is oxidized by reduction of the acid protons of the sulphamic acid without adding special oxidization means. The nickel sulphamate contained in an aqueous solution is especially suitable for electroplating technology since it is for the most part free of foreign ions and amorphous nickel sedimentations.

L'invention concerne un procédé permettant de produire du sulfamate de nickel par réaction de nickel élémentaire avec de l'acide sulfamique. Le nickel est désintégré par une forte agitation, mise en suspension ou dispersion du mélange nickel-acide au moyen d'un outil d'agitation, de mise en suspension ou de dispersion, dont le but est d'introduire une haute densité d'énergie dans ledit mélange de réaction. Le nickel est oxydé par réduction des protons de l'acide sulfamique, sans addition d'agents d'oxydation spéciaux. Le sulfamate de nickel contenu dans une solution aqueuse convient particulièrement à une utilisation dans les technologies de galvanoplastie puisqu'il est en majeure partie exempt d'ions étrangers et de sédiments de nickel amorphe.

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