Method and devices for producing air sensitive electrode...

C - Chemistry – Metallurgy – 22 – F

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C22F 1/16 (2006.01) H01M 4/139 (2010.01)

Patent

CA 2705260

A unit for use within a furnace which is absent a controlled atmosphere, for carrying out a synthesizing process for synthesizing precursors to form a synthesized product at elevated temperatures. The unit consists of a vessel, having at least one opening, for containing materials of the synthesizing process, and a solid reductive material. The materials of the synthesizing process are separated from the atmosphere of the furnace by either the vessel or the reductive material. The unit is especially suited for synthesizing LiFePO4 from Fe2O3, Li2CO3, carbon black, and phosphoric acid precursors.

L'invention concerne une unité destinée à être utilisée dans un four à atmosphère non contrôlée pour conduire une opération de synthèse de précurseurs en vue de former un produit de synthèse à hautes températures. Cette unité est constituée d'une cuve qui présente au moins une ouverture et qui est destinée à contenir les matériaux de l'opération de synthèse, ainsi que d'un matériau réducteur solide. Les matériaux de l'opération de synthèse sont séparés de l'atmosphère du four par la cuve ou par le matériau réducteur. L'unité convient particulièrement bien pour synthétiser LiFePO4 à partir de Fe2O3, Li2CO3, de noir de carbone et de précurseurs d'acide phosphorique.

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