Method and instrument for low temperature microwave assisted...

Details Method and instrument for low temperature microwave assisted... Method and instrument for low temperature microwave assisted...

B - Operations, Transporting

01

J

B01J 19/12 (2006.01) H05B 6/80 (2006.01)

Patent

CA 2512941

An instrument and associated method are disclosed for performing microwave assisted organic chemical synthesis at low temperatures. The instrument includes a reaction vessel formed of a microwave transparent material that defines an interior reaction chamber for carrying out microwave assisted reactions in the chamber, a cooling jacket immediately surrounding the reaction vessel for cooling the vessel and the vessel contents during the application of microwave energy to contents in the vessel when a microwave transparent media used as a fluid coolant is present in the jacket. The instrument includes means for supplying a microwave transparent fluid coolant to the cooling jacket and means for venting the fluid coolant from the cooling jacket, a fluid coolant reservoir in communication with the cooling jacket, and a pump in communication with the reservoir and the cooling jacket for circulating fluid coolant from the fluid coolant reservoir through the cooling jacket and around the reaction vessel.

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