Method and reagent composition for subtyping lymphocytes in...

G - Physics – 01 – N

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G01N 35/00 (2006.01) G01N 33/49 (2006.01) G01N 33/569 (2006.01) G01N 33/577 (2006.01) G01N 33/80 (2006.01)

Patent

CA 2070244

ABSTRACT A rapid method for detection of monoclonal antibody labeled cells using forward light scatter/absorption clinical flow cytometers is disclosed. Calf-intestinal alkaline phosphatase is conjugated to mouse monoclonal antibodies (anti-CD2, CD3, CD4, CD8, CD19) for direct immunoenzymatic labeling. Red cells are pre-conditioned for lysis during the first incubation period with the alkaline phosphatase conjugated monoclonal antibodies by ammonium-sulfate which is followed by an early fixation of white cells in the presence of dextrose. The combination of 5-bromo-4-chloro-3-indolyl phosphate and nitroblue-tetrazolium salt in diethanolamine buffer, containiny zinc glycinate, at pH 9.5?0.1, is used as a buffer/substrate to yield stable, insolu- ble and intense purplish precipitates on the surface of the cells labeled with alkaline phosphatase conjugated monoclonal antibodies. The separation of granulocytes and lymphocytes is detected by a forward light scatter/absorption optics. Endoge- nous alkaline phosphatase in granulocytes is inhibited with levamisole. Early mild ixation of the white cells permits incubation at 35°C to 40°C which accelerates each step of the reaction without disrupting the cells throughout the procedure, making the procedure adaptable for use on automated cytometric instrumentation. 1515S

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