Method for adjusting the magic angle in nmr experiments

G - Physics – 01 – R

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324/1

G01R 33/30 (2006.01)

Patent

CA 1157521

A METHOD FOR ADJUSTING THE MAGIC ANGLE IN NMR EXPERIMENTS Abstract A method for adjusting the orientation of the rotation axis for a sample in a nuclear magnetic resonance (NMR) experiment includes using a field gradient in a specific direction with respect to the external magnetic field of the NMR experiment to establish a calibrated reference direction with which the rotation axis may be aligned. Preferably, the magnetic field gradient is at an angle of 54.7°. A preferred embodiment of this invention includes automatic control steps in the method.

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