Method for brevicomin synthesis and use in beetle control

Details Method for brevicomin synthesis and use in beetle control Method for brevicomin synthesis and use in beetle control

C - Chemistry, Metallurgy

07

D

260/353.8

C07D 493/08 (2006.01)

Patent

CA 1271483

ABSTRACT OF THE DISCLOSURE A process for the production of the beetle aggregation pheromone brevicomin comprising reacting acrolein dimer sequentially with ethyllithium, a methylating agent and aqueous protonic acid. In a modification of the process the acrolein dimer is reacted with ethyl Grignard reagent prior to reaction with an alkyllithiun compound. The process includes distributing the brevicomin product to areas to be controlled for beetles.

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