Method for crystallization of...

C - Chemistry – Metallurgy – 07 – K

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C07K 5/075 (2006.01) C07K 1/14 (2006.01) C07K 5/072 (2006.01)

Patent

CA 2081869

A method of crystallizing ~-L-aspartyl-L- phenylalanine methyl ester comprises cooling a crystal- lizing solution of ~-L-aspartyl-L-phenylalanine methyl ester by indirect heat exchange with a coolant, the crystallizing solution of ~-L-aspartyl-L-phenylalanine methyl ester having a temperature no more than 20°C higher than the temperature of the coolant, stirring the crystallizing solution of ~-L-aspartyl-L-phenylalanine methyl ester and circulating the coolant while continu- ously feeding an aqueous solution of ~-L-aspartyl-L- phenylalanine methyl ester to the crystallizing solution of ~-L-aspartyl-L-phenylalanine methyl ester. The method of the invention enables one to reduce the amount of scale deposited on heat transfer surfaces of crystallizers.

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