Method for determination of cholesterol in high-density...

C - Chemistry – Metallurgy – 12 – Q

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C12Q 1/26 (2006.01) C12Q 1/44 (2006.01) G01N 33/92 (2006.01)

Patent

CA 2605329

Disclosed are a method for determination of HDL cholesterol, a reagent for the determination and a kit for the determination which realize a convenient and accurate determination of HDL cholesterol. A method for determination of cholesterol in a high-density lipoprotein in a sample, the method comprising the steps of reacting the sample with i) a cholesterol ester hydrolase and a cholesterol oxidase or ii) a cholesterol ester hydrolase, an oxidized coenzyme and a cholesterol dehydrogenase in an aqueous medium containing a specific nitrogenated surfactant having a structure of an amine or ammonium salt and a polyanion to produce hydrogen peroxide or a reduced coenzyme, and determining hydrogen peroxide or the reduced coenzyme.

L~invention dévoile un procédé de détermination du cholestérol des LPHD, un réactif pour cette détermination et un kit permettant de déterminer de manière pratique et précise le cholestérol des LPHD. Le procédé de détermination du cholestérol dans une lipoprotéine de haute densité d~un échantillon comprend les étapes consistant à faire réagir l~échantillon avec i) une cholestérol ester hydrolase et une cholestéroloxydase ou ii) une cholestérol ester oxydase, une coenzyme oxydée et une cholestérol déshydrogénase, dans un milieu aqueux contenant un surfactant azoté spécifique à la structure d~un sel aminé ou ammonium et un polyanion, afin de produire du péroxyde d~hydrogène ou une coenzyme réduite et à identifier le peroxyde d~hydrogène ou la coenzyme réduite.

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