Method for measuring degree of cure of resin in a composite...

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Details

IPC codes

G01N 21/35 (2006.01) G01N 21/31 (2006.01) G01N 33/44 (2006.01) H05K 3/02 (2006.01)

Type

Patent

Patent number

CA 2068419

Description

A method for measuring the degree of cure of a resin in a composite material such as a prepreg employs an infrared spectrometer device having means for resolving specific frequency absorbance information and means for providing a quantitative spectral analysis of the amount of energy absorbed at first and second frequencies of radiation which are characteristic of unreactive and cure-reactive groups, respectively, contained in the resin. The method comprises irradiation of the composite material with the infrared light source, generating a quantitative spectral analysis of the amount of energy absorbed at the first and second frequencies determining the height of or area under the spectrum maximum at each of the first and second frequencies, and calculating a ratio of one of the determined values to the other to provide a measurement of the degree of cure of the resin.

Procédé permettant de vérifier le degré de prise de la résine dans un matériau composite, par exemple un tissu préimprégné, et mettant en oeuvre un spectromètre à infrarouge capable de résoudre les fréquences spécifiques d'absorption et de faire une analyse spectrale quantitative de l'énergie absorbée aux fréquences spécifiques des groupes réactifs et non réactifs à la prise dans la résine. Le procédé consiste à soumettre le matériau composite aux radiations infrarouges, lancer une analyse spectrale quantitative pour déterminer la quantité d'énergie absorbée aux première et deuxième fréquences, déterminer la hauteur des pics ou la superficie sous les pics à la première et à la deuxième fréquences, et calculer le rapport entre les deux valeurs déterminées pour obtenir une mesure du degré de prise de la résine.

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