Method for preparing 3-ethylbenzophenone

C - Chemistry – Metallurgy – 07 – C

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260/578.1

C07C 49/784 (2006.01) C07C 2/68 (2006.01) C07C 45/28 (2006.01) C07C 45/64 (2006.01) C07C 45/82 (2006.01) C07C 45/85 (2006.01) C07C 51/12 (2006.01)

Patent

CA 1267658

ABSTRACT OF THE DISCLOSURE The present invention provides a method for preparing 3-ethylbenzophenone in a high purity which comprises the steps of alkylating benzene with ethylene in the presence of an alkylating catalyst to obtain an alkylated product composed mainly of unreacted benzene, ethylbenzene, poly- ethylbenzenes and heavier substances; subjecting the alkylated product to rectification in order to recover therefrom a fraction which has a temperature range of boiling points within the range of 275 to 310°C (in terms of atmospheric pressure); heating the recovered fraction together with a mixture of nitric acid and water; carrying out purification, if necessary; and performing distillation to recover therefrom 3-ethylbenzophenone represented by the formula (I): Image . . . ( I )

517937

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