Method for preparing improved porous metal-hydride compacts...

C - Chemistry – Metallurgy – 01 – B

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18/1122, 23/293

C01B 6/02 (2006.01) B22F 3/00 (2006.01) B22F 3/11 (2006.01) C01B 3/00 (2006.01)

Patent

CA 1193820

METHOD FOR PREPARING IMPROVED POROUS METAL-HYDRIDE COMPACTS AND APPARATUS THEREFOR ABSTRACT OF THE DISCLOSURE The present invention relates to a method and apparatus for preparing metal-embedded porous metallic-hydride (pmh) compacts capable of withstanding repeated hydriding - dehydriding cycles without disintegrating. According to the invention, the finely divided hydridable metal alloy hydride is admixed with a finely divided metal selected from Al, Ni, Cu or other transition metals and charged with hydrogen. The resulting mixture is sintered in a furnace in which hydrogen is introduced at a pressure above the equilibrium pressure to the prevailing temperature, mechanical stress being applied simultaneously. The compacts obtained possess outstanding stability r as shown by the fact that they have remained intact even after more than 6000 cycles.

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