Method for preparing purified terephthalic acid and...

C - Chemistry – Metallurgy – 07 – C

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C07C 51/43 (2006.01) C07C 63/24 (2006.01) C07C 63/26 (2006.01)

Patent

CA 2333706

A method and apparatus for preparing purified terephthalic acid and, optionally, isophthalic acid from mixed xylenes. The method of the present invention purifies the oxidation reactor effluent containing a mixture of terephthalic acid and isophthalic acid as well as minor amounts of 4- carboxybenzaldehyde (4-CBA), 3-carboxybenzaldehyde (3-CBA), and toluic acid isomers, to produce purified terephthalic acid and, optionally purified isophthalic acid in an integrated process.

L'invention se rapporte à un procédé et à un appareil de préparation d'acide téréphtalique et, éventuellement, d'acide isophtalique purifiés à partir de mélanges de xylènes. Ledit procédé consiste à purifier l'effluent du réacteur d'oxydation, qui contient un mélange d'acide téréphtalique et d'acide isophtalique ainsi que de faibles quantités de 4-carboxybenzaldéhyde (4-CBA), de 3-carboxybenzaldéhyde (3-CBA) et d'isomères de l'acide toluique, de manière à produire de l'acide téréphtalique purifié et, éventuellement, de l'acide isophtalique purifié, au cours d'un processus intégré.

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