Method for producing a packing structure with control over...

C - Chemistry – Metallurgy – 04 – B

Patent

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C04B 2/10 (2006.01) C04B 28/18 (2006.01)

Patent

CA 2729179

The invention relates to a method for producing a packing structure, characterised in that it includes the following steps: a) a step in which the temperature of an initial mixture of quicklime and silica is raised to a temperature T1 of between 150 and 300°C over a period of less than 10 hours; b) a step in which hydrothermal synthesis is performed using the mixture of quicklime and silica produced in step (a) at a temperature T1 of between 150 and 300°C and at a pressure P1 of between 5.105 Pa and 25.105 Pa over a period t1 of between 10 and 70 hours; c) a step in which the mixture produced in step (b) is cooled from temperature T1 to ambient temperature over a period of between 1 and 48 hours at a cooling rate ?TR1 of between 3 and 200°C / hour; and d) a step in which the mixture produced in step (c) is dried.

Procédé de fabrication d'une structure de garnissage, caractérisé en ce qu'il comprend les étapes suivantes : a) une étape de montée en température, sur une durée inférieure à 1Oh, d'un mélange initial de chaux vive et de silice à une température T1 comprise entre 150 et 300°C, b) une étape de synthèse hydrothermale effectuée : à partir du mélange de chaux vive et de silice issu de l'étape a); à une température T1 comprise entre 150 et 300°C; à une pression P1 comprise entre 5.10 5 Pa et 25.10 5 Pa; et pendant une durée tl comprise entre 10h et 70h; c) une étape de refroidissement, sur une durée comprise entre 1 et 48 h, du mélange issu de l'étape b) de la température T1 à la température ambiante à une vitesse de refroidissement 4TR1 comprise entre 3 et 200°C / heure. d) une étape de séchage du mélange issu de l'étape c).

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