Method for producing gaseous diazoalkanes

Details Method for producing gaseous diazoalkanes Method for producing gaseous diazoalkanes

C - Chemistry, Metallurgy

07

C

C07C 245/16 (2006.01)

Patent

CA 2570808

The invention relates to a method for producing diazoalkanes, which is characterized by dissolving a diazoalkane precursor in a first solvent, dissolving a base in a second solvent, allowing the substances to react in a reactor while forming the diazoalkane and removing the diazoalkane under reduced pressure. The inventive method is especially suitable for producing diazomethane.

L'invention concerne un procédé de fabrication de diazoalcanes consistant à dissoudre un précurseur de diazoalcane dans un premier solvant, à dissoudre une base dans un deuxième solvant, à faire réagir ces produits dans un réacteur de manière à former le diazoalcane et à évacuer le diazoalcane obtenu sous pression réduite. Le procédé selon l'invention est particulièrement adapté à la fabrication de diazométhane.

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