Method for production of nanofibres

D - Textiles – Paper – 01 – D

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D01D 5/00 (2006.01) D01D 5/06 (2006.01) D01F 4/00 (2006.01) D01F 9/00 (2006.01)

Patent

CA 2702368

The invention relates to the method for production of nanofibres through electrostatic spinning of polymer matrices prepared upon biopolymers of chitosan or collagen. The biopolymer before spinning is dissolved as clean or in mixture with auxiliary non-toxic polymer in solvent system, which comprises an organic or inorganic acid, selected from the group of acetic acid in concentration from 30 % to 90 % of weight, lactic acid, malic acid, trihydrogen-phosphoric acid and their mixtures, and this solution is brought into electrostatic field between the spinning electrode and collecting electrode, while the produced biopolymer nanofibres comprise more than 90 % of weight of biopolymer in dry mass.

L'invention concerne un procédé de production de nanofibres par filage électrostatique de matrices polymères préparées sur des biopolymères de chitosane ou de collagène. Avant le filage, le biopolymère est dissous sous forme pure ou en mélange avec un polymère non toxique auxiliaire dans un système de solvants renfermant un acide organique ou inorganique choisi dans le groupe constitué par l'acide acétique en concentration comprise entre 30% et 90% en poids, l'acide lactique, l'acide malique, l'acide trihydrogène-phosphorique et leurs mélanges, cette solution étant acheminée dans un champ électrostatique entre l'électrode de filage et l'électrode de collecte, les nanofibres biopolymères produites comprenant plus de 90% en poids de biopolymère en masse sèche.

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