Method for purification of ethylene glycol

C - Chemistry – Metallurgy – 07 – C

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260/641.4

C07C 29/76 (2006.01) C07C 31/20 (2006.01)

Patent

CA 1330350

METHOD FOR PURIFICATION OF ETHYLENE GLYCOL Abstract of the Disclosure The invention discloses a method for purifying ethylene glycol by using an ion exchange resin. The anion exchange resin adsorbs aldehyde impurities from the ethylene glycol. A basic anion exchange resin is prepared in a bisulfite or a hydroxyl form. The ethylene glycol passed through the column under air or nitrogen gas atmospheric conditions. As a result, aldehydes are absorbed as their bisulfite adducts. Subsequently, the ethylene glycol may be treated by carbon adsorption to improve the UV/visible absorbance. A weakly basic resin such as Amberlte? IR-45 is preferred, but other anion exchange resins are also expected to be effective.

547209

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