Method for rapidly obtaining crystals with desirable...

C - Chemistry – Metallurgy – 12 – N

Patent

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C12N 9/54 (2006.01) C07K 1/30 (2006.01) C30B 7/00 (2006.01)

Patent

CA 2361507

The present invention provides a crystallization process wherein a starting temperature is selected such that a desirable crystal morphology (e.g., square) is obtained. A temperature shift is then introduced, providing that the shift is not enough to induce further nucleation, where the crystals continue to grow in the desirable fashion, but with different kinetics, e.g., a higher rate of crystallization. As a result, the process gives a crystalline product with desirable morphology at a higher crystallization rate.

La présente invention concerne un procédé de cristallisation selon lequel une température de base est sélectionnée de manière à obtenir un cristal avec une morphologie désirée (par exemple carrée). Un changement de température est alors introduit, dans la mesure où ce changement ne suffit pas à induire une plus grande nucléation, où les cristaux continuent de s'agrandir de la manière désirée mais avec une cinétique différente, par exemple un taux de cristallisation plus élevé. On obtient avec ce procédé un produit cristallin à la morphologie désirée et au taux de cristallisation plus élevé.

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