Method for the continuous production of...

C - Chemistry – Metallurgy – 08 – G

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C08G 63/78 (2006.01) C08G 63/183 (2006.01)

Patent

CA 2378649

The invention relates to a method for the continuous production of polybutyleneterephthalate from terephthalic acid and 1,4-butanediol, comprising the following: d) the direct esterification of terephthalic acid with 1,4-butanediol in a reactor series consisting of at least two reactors; e) the precondensation of the product of esterification obtained in step a); f) the polycondensation of the precondensate obtained in step b). The reactor series in step a) is operated with a falling reaction pressure and a non- rising temperature.

L'invention concerne un procédé de production continue de polybutylèntéréphthalat à partir d'acide téréphathalique et de 1,4-butandiol. Ce procédé consiste à effectuer: d) l'estérification directe de l'acide téréphthalique avec 1,4-butandiol dans un réacteur en cascade constitué d'au moins deux réacteurs, e) la précondensation du produit d'estérification obtenu en a) ; f) la polycondensation du précondensat obtenu en b). A l'étape a), le réacteur en cascade fonctionne avec une pression décroissante et une température non croissante.

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