Method for the preparation of polymeric micelle via phase...

A - Human Necessities – 61 – K

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A61K 47/30 (2006.01) A61K 9/107 (2006.01) A61K 9/19 (2006.01)

Patent

CA 2408548

A method for preparing a biodegradable polymeric micellar composition using liquid polyethylene glycol as a phase separation medium comprising mixing an effective amount of a hydrophobic drug, an amphiphilic block copolymer and a phase separation medium comprising liquid poly(ethylene glycol), stirring and heating to give a solution; cooling and stirring the solution until it forms a polymeric micelle by phase separation; diluting the polymeric micelle solution in distilled water and then dialyzing it against excess water to remove the liquid polyethylene glycol; and freeze-drying the dialyzed aqueous solution to give a polymeric micellar composition in a powdered state.

L'invention concerne un procédé de préparation d'une composition micellaire polymère biodégradable mettant en oeuvre du polyéthylène glycol liquide en tant que milieu de séparation de phases. Ce procédé comprend les étapes consistant à mélanger une quantité efficace d'un médicament hydrophobe, un copolymère séquencé amphiphile et un milieu de séparation de phases comprenant un polyéthylène glycol liquide, à agiter et à chauffer ceci de manière à obtenir une solution; à refroidir et à agiter la solution jusqu'à ce qu'elle forme une micelle polymère par séparation de phases; à diluer la solution micellaire polymère dans de l'eau distillée et puis à la dialyser contre un excès d'eau en vue d'éliminer le polyéthylène glycol liquide; et à lyophiliser la solution dialysée aqueuse de manière à obtenir une composition micellaire polymère sous forme de poudre.

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