Method for the preparation of trinuclear molybdenum-sulfur...

Details Method for the preparation of trinuclear molybdenum-sulfur... Method for the preparation of trinuclear molybdenum-sulfur...

C - Chemistry, Metallurgy

07

F

C07F 11/00 (2006.01) C10M 135/18 (2006.01) C10M 137/10 (2006.01) C10M 159/18 (2006.01)

Patent

CA 2313408

Oil-soluble or oil-dispersible trinuclear molybdenum-sulfur compounds are made by reacting less than three, such as 1.5 to 2.5, preferably 2 to 2.1, molar equivalents of a disulfide with one molar equivalent of a compound containing the [Mo3S13]2-ion. The trinuclear compounds include S-containing ligands that are derived from the disulfide reactant via cleavage of the disulfide bond; the ligands are bound to the core via the S atoms.

On a produit des composés trinucléaires de molybdène-soufre solubles dans l'huile ou dispersables dans l'huile en faisant réagir moins de 3, tel que 1,5 à 2,5, de préférence 2 à 2,1 équivalents molaires d'un disulfure avec un équivalent molaire d'un composé contenant l'ion [Mo¿3?S¿13?]?2-¿. Les composés trinucléaires comprennent des ligands contenant S lesquels sont dérivés du réactif disulfure par clivage de la liaison disulfure; les ligands sont liés au noyau par les atomes S.

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