Method for the purification of biological macromolecules

C - Chemistry – Metallurgy – 12 – N

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C12N 15/09 (2006.01) G01N 33/561 (2006.01)

Patent

CA 2717308

Disclosed are methods and devices for electrophoretic separation of free biomolecules from molecular complexes comprising biomolecules of interest during which inhomogeneity in the molecular complexes is masked. The methods can include loading a sample which contains free biomolecules and the complexes that include biomolecules of interest to a proximal end of an electrophoresis gel. The sample is electrophoresed for a period of time sufficient for the free biomolecules to elute off a distal end of the gel while the molecular complexes that include the biomolecules of interest are retained in the electrophoresis gel, thereby separating the molecular complexes from the free biomolecules. The direction of electrophoresis is reversed and the sample is electrophoresed for a period of time sufficient for the molecular complexes of bound biomolecules of interest to elute from the proximal end of the electrophoresis gel.

La présente invention concerne des procédés et des dispositifs de séparation électrophorétique de biomolécules libres de complexes moléculaires, qui comprennent des biomolécules dintérêt, durant lesquels la non-homogénéité des complexes moléculaires est masquée. Le procédé peut comprendre le chargement dun échantillon qui contient des biomolécules libres et les complexes qui comprennent les biomolécules dintérêt à une extrémité proximale dun gel délectrophorèse. Léchantillon est alors soumis à une électrophorèse pendant une durée suffisante pour lélution des biomolécules libres dune extrémité distale du gel alors que les complexes macromoléculaires qui comprennent les biomolécules dintérêt sont retenus dans le gel délectrophorèse, séparant ainsi les complexes moléculaires des biomolécules libres. La direction de lélectrophorèse est inversée et léchantillon est soumis à une électrophorèse pendant une durée suffisante pour lélution des complexes moléculaires de biomolécules liées dintérêt de lextrémité proximale du gel délectrophorèse.

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