Method of making high purity dense silica of large particle...

C - Chemistry – Metallurgy – 01 – B

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C01B 33/18 (2006.01) C01B 33/16 (2006.01) C03C 1/00 (2006.01)

Patent

CA 1318481

88-3-434 CN METHOD OF MAKING HIGH PURITY DENSE SILICA OF LARGE PARTICLE SIZE Abstract A method of making high purity, dense silica of large particle size is described. Tetraethylorthosilicate is mixed with ethanol and is added to a dilute acid solution having a pH of about 2.25. The resulting solution is digested for about 5 hours, then 2N ammonium hydroxide is added to form a gel at a pH of 8.5. The gel is screened through an 18-20 mesh screen, vacuum baked, calcined in an oxygen atmosphere and finally heated to about 1200°C in air to form a large particle size, high purity, dense silica.

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