Method of mycophenolate mofetil preparation

Details Method of mycophenolate mofetil preparation Method of mycophenolate mofetil preparation

C - Chemistry, Metallurgy

07

D

C07D 413/02 (2006.01) C07D 307/88 (2006.01)

Patent

CA 2450013

Synthesis of mycophenolate mofetil (1), where R1=2-(-morpholinyl)ethyl and R2=hydrogen atom, includes reaction of mycophenolic acid with 4-(2- hydroxyethyl)morpholine in a suitable solvent under azeotropic separation of water.

L'invention concerne la synthèse de mofétilmycophénolate (1), où R?1¿représente 2-(-morpholinyl)éthyle et R?2¿ représente un atome d'hydrogène. Cette synthèse comprend la réaction d'acide mycophénolique avec de la 4-(2-hydroxyéthyl)morpholine dans un solvant approprié dans des conditions de déshydratation azéotropique.

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