Method of nitriding refractory metal articles

C - Chemistry – Metallurgy – 23 – C

Patent

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C23C 16/34 (2006.01) C04B 41/85 (2006.01) C23C 8/24 (2006.01) C23C 16/46 (2006.01) H05B 6/64 (2006.01)

Patent

CA 2078120

2078120 9116801 PCTABS00008 A method of nitriding an article of refractory-nitride-forming metal or metalloids is described. A consolidated metal or metalloid article is placed inside a microwave oven and nitrogen containing gas is introduced into the microwave oven. The metal or metalloid article is heated to a temperature sufficient to react the metal or metalloid with the nitrogen by applying a microwave energy within the microwave oven. The metal or metalloid article is maintained at that temperature for a period of time sufficient to convert the article of metall or metalloid to an article of refractory nitride. In addition, a method of applying a coating, such as coating of an oxide, a carbide, or a carbo-nitride, to an article of metal or metalloid by microwave heating is described.

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