Method of pan granulation

B - Operations – Transporting – 01 – J

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B01J 2/14 (2006.01) C05C 1/02 (2006.01) C05G 3/00 (2006.01)

Patent

CA 1063778

Method of Pan granulation Abstract of Disclosure The invention provides an improved pan granulation process for the production of low-water or substantilly an- hydrous nitrogenous compounds. Hot nitrogenous melt and cooled particulate solids are fed to a rotating pan to form a crescent-shaped bed of rolling or tumbling particles, the thickness or depth of the bed increasing in the direction towards the periphery of the pan and its overflow sector, i.e. position 2 o'clock to position 6 o'clock when the pan surface is regarded as a clock face and the rotation of the pan is counter-clockwise; according to the invention the cooled solid particles are fed to the pan at a point where the depth of existing material is small, desirably substantially zero, preferably in position 7 to 8 o'clock, if need be by feeding the particles through a tube or the like which extends into the tumbling material on the pan to the proximity of the sur- face of the pan itself. Subsequently, the cooled particles will then be covered by warmer particles tumbling over them. Further, the temperature of the product material as dischar- ged from the pan is controlled to and maintained at about 4 to 25°C below the melting point of the material, and the main part of the melt is sprayed on to the surface of the bed within a zone in the quadrant 12 to 3 o'clock where the coarser particles appear, whereby the highest temperature of the bed will be restricted to a surface layer within this zone.

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