Method of preparing manganese oxide octahedral molecular sieve

Details Method of preparing manganese oxide octahedral molecular sieve Method of preparing manganese oxide octahedral molecular sieve

B - Operations, Transporting

01

J

B01J 20/04 (2006.01) C01B 39/00 (2006.01) C01G 45/02 (2006.01)

Patent

CA 2160511

Manganese oxide octahedral molecular sieve (OMS) is produced by the method comprising: a) forming an aqueous reaction medium containing manganese cation and permanganate anion, the reaction medium being maintained at a pH of not greater than about 4.5; b) refluxing the aqueous reaction medium under conditions which are effective to produce solid crystalline manganese oxide octahedral molecular sieve product; and, c) recovering the solid crystalline product. The method of this invention is carried out in an open system, i.e., a reflux condenser, and results in the formation of OMS which is thermally stable up to about 600°C.

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