Method of preparing trialkyl-tin hydrides

Details Method of preparing trialkyl-tin hydrides Method of preparing trialkyl-tin hydrides

C - Chemistry, Metallurgy

07

F

C07F 7/22 (2006.01)

Patent

CA 2098213

The invention concerns a method of preparing trialkyl-tin hydrides by a process that ensures outstanding long-term stability. bis-[Trialkyl-tin) oxides are dissolved in a solvent that mixes only to some extent if at all with water and converted with an aqueous solution of sodium borohydride stabilized with a base. The product is obtained by phase separation and optionally by distillation. The trialkyl-tin hydride is obtained almost quantitatively with a yield of more than 95 %.

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