C - Chemistry – Metallurgy – 01 – B
Patent
C - Chemistry, Metallurgy
01
B
23/74
C01B 25/20 (2006.01) C01B 25/16 (2006.01) C01B 25/24 (2006.01)
Patent
CA 1135027
43-4578A METHOD OF PREPARING ULTRAPHOSPHORIC ACID ABSTRACT Ultraphosphoric acid containing a phosphorus to hydrogen ratio of greater than 1 can be prepared by bringing together in a reaction zone elemental phos- phorus and a sufficient amount of oxygen in a free- oxygen containing gas to form phosphorus pentoxide, and a sufficient amount of water to form ultraphos- phoric acid. The mole ratio of water to phosphorus pentoxide is maintained less than 1:1. Heat is removed from the product stream of the reaction zone to condense at least some of the ultraphosphoric acid which is then collected. In the preferred embodi- ment, a heat exchange fluid such as pressurized water is circulated through a cooling coil positioned to remove heat from the product stream of the reaction zone. The ultraphosphoric acid can be combined with water to provide polyphosphoric acid.
375027
Mcfadden Fincham
Solutia Inc.
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