Method of producing an n-(substituted) morpholine compound

Details Method of producing an n-(substituted) morpholine compound Method of producing an n-(substituted) morpholine compound

C - Chemistry, Metallurgy

07

D

260/247.5

C07D 265/30 (2006.01) C07D 295/00 (2006.01)

Patent

CA 1092114

METHOD OF PRODUCING AN N-(SUBSTITUTED) MORPHOLINE COMPOUND (D#75,011-2-F) Abstract of the Disclosure An improved process for selectively producing an N-(substituted)morpholine compound is disclosed wherein an oxydialkanol compound is contacted with a primary amine in the presence of a catalytically effective amount of a phosphorus- containing substance at a temperature of from about 220°C to about 350°C under a pressure sufficient to maintain the mixture essentially in liquid phase, said N-(substituted) morpholine compound produced having the formula: Image wherein each R is, independently, hydrogen or a lower alkyl radical and R' is an alkyl radical, a substituted alkyl radical, an aryl radical or a substituted aryl radical; and, recovering from the resultant reaction mixture said N-(substituted) morpholine compound.

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