Method of producing n-benzyloxycarbonyl-l-aspartic acid

Details Method of producing n-benzyloxycarbonyl-l-aspartic acid Method of producing n-benzyloxycarbonyl-l-aspartic acid

C - Chemistry, Metallurgy

07

K

260/468.1

C07K 5/075 (2006.01)

Patent

CA 1155453

ABSTRACT OF THE DISCLOSURE The reaction between L-aspartic acid and benzyloxy- carbonyl chloride is carried out at a specific pH range, i.e., 12.0 to 13.5, whereby highly pure N-benzyloxycarbonyl- L-aspartic acid can be obtained in high yields, while both the formation of by-product N-benzyloxycarbonyl-?- or .beta.-L-aspartyl-L-aspartic acid and the decomposition of benzyloxycarbonyl chloride to benzyl alcohol are suppressed; the resulting N-benzyloxycarbonyl-L-aspartic acid is useful as a sweetener.

369775

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