Method of recovering molybdenum oxide

C - Chemistry – Metallurgy – 01 – G

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C01G 39/02 (2006.01) C22B 34/34 (2006.01)

Patent

CA 1164629

ABSTRACT OF THE DISCLOSURE A method of recovering molybdenum oxide by oxidation of a molybdenum sulfide concentrate contaminated with impurities wherein the concentrate having an average particle size in the range of 20 to 90 microns is suspended to form an aqueous suspension which is oxidized at elevated temperature and elevated oxygen partial pressure in an autoclave, The suspension withdrawn from the autoclave is filtered to remove the molybdenum oxide from the primary filtrate containing sulfuric acid and this filtrate is neutralized with lime to form calcium sulfate which is then removed from the suspension to provide a second filtrate. According to the invention, only the second filtrate is recirculated at a rate such that the suspension density in the oxidation stage is between 100 to 150 g of solids per liter and this suspension density is maintained in the oxidation stage by the recirculation.

407785

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