Method of separating dinitrogen pentoxide from its solution...

C - Chemistry – Metallurgy – 25 – B

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C25B 1/00 (2006.01) C01B 21/20 (2006.01)

Patent

CA 2049014

A method of separating N2O5 from its solution in nitric acid which comprises the steps of: (a) preparing, by the electrochemical oxidation of N2O4 in nitric acid, a nitric acid solution at a temperature of at least 10 °C containing at least 45 wt % of dissolved (N2O4 + N2O5) and having a dissolved N2O5: nitric acid ratio by weight of at least 1:3; and (b) cooling the acid solution to less than 8 °C until an N2O5 solvate precipitates froze solution. The main advantage of the invention is that it enables electrically-efficient electrochemical methods to be employed in the production of the acid solution from which the solute is recovered.

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