C - Chemistry – Metallurgy – 23 – C
Patent
C - Chemistry, Metallurgy
23
C
C23C 8/24 (2006.01) A61F 2/28 (2006.01) A61F 2/30 (2006.01) A61L 27/00 (2006.01) A61F 2/00 (2006.01) A61F 2/36 (2006.01)
Patent
CA 2049809
A method of surface hardening titanium orthopedic implant devices, and a titanium orthopedic implant device prepared by the disclosed method. An orthopedic implant device made of pure titanium or a titanium alloy, such as Ti-6Al-4V (ELI) is exposed to molecular nitrogen gas at a process temperature and for a process time duration sufficient to enhance surface hardness and wear resistance properties, without the formation of a measurable TiN layer that tends to increase surface roughness and diminish wear resistance properties. The process temperature is in the range of 750°F, to 1300°F., preferably about 1100°F, and the process time duration at the preferred process temperature is approximately 8 hours. The hardened surface of the titanium implant occurs primarily due to solid solution hardening of the titanium with nitrogen by dissolution.
Crowninshield Roy D.
Ottersberg Walter H.
Parr Jack E.
Shetty H. Ravindranath
Bristol-Myers Squibb Company
Gowling Lafleur Henderson Llp
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