Method of technical cumene hydroperoxide acidic cleavage to...

C - Chemistry – Metallurgy – 07 – C

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C07C 39/04 (2006.01) C07C 37/08 (2006.01) C07C 45/53 (2006.01) C07C 49/08 (2006.01)

Patent

CA 2143578

Technical cumylhydroperoxide of a wide composition range is cleaved in circulating reactors of a shell and tube design at the same elevated pressure as dicumyl peroxide is cleaved in a plug flow reactor with a recirculation ratio of at least 26. The cleavage process is controlled using two calorimeters and controlling the absolute .DELTA. T value which is thedifference in the temperature drop between the two calorimeters.

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