Methyl chloroformate process

C - Chemistry – Metallurgy – 07 – C

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260/467

C07C 69/96 (2006.01) C07C 68/02 (2006.01)

Patent

CA 1094093

B/1089 METHYL CHLOROFORMATE PROCESS Abstract of The Disclosure A continuous process for producing high-purity methyl chloroformate, by reacting liquid methanol with an excess of phosgene at no more than 20°C., preferably about 15°C. Phosgene is absorbed in a large circulating load of pre-formed chloro- formate that has also had methanol added to it. The product stream is treated to remove light ends, and a 98% pure product results.

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