Microwave assisted continuous synthesis of nanocrystalline...

B - Operations – Transporting – 22 – F

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B22F 9/20 (2006.01) B22F 1/00 (2006.01) B22F 9/00 (2006.01) C21C 1/04 (2006.01) C22B 5/20 (2006.01) C22C 1/04 (2006.01)

Patent

CA 2515042

A method of forming a nanocrystalline metal, comprising the steps of: providing a reaction mixture comprising a metal precursor and an alcohol solvent; continuously flowing the reaction mixture through a reactor; applying microwave or millimeter-wave energy to the reaction mixture; wherein the microwave or millimeter-wave energy is localized to the vicinity of the reaction mixture; and heating the reaction mixture with the microwave or millimeter-wave energy so that the alcohol solvent reduces the metal precursor to a metal; wherein the heating occurs in the reactor.

L'invention concerne un procédé de formation d'un métal nanocristallin. Ce procédé comprend les étapes consistant: à utiliser un mélange de réaction comprenant un précurseur métallique et un solvant alcoolique; à faire couler en continu ledit mélange de réaction dans un réacteur; à appliquer des micro-ondes ou une énergie à ondes millimétriques sur le mélange de réaction, ces dernières étant localisées à proximité dudit mélange de réaction; et à chauffer ledit mélange de réaction au moyen desdites micro-ondes ou de ladite énergie à ondes millimétriques afin que le solvant alcoolique réduise le précurseur métallique en métal, le chauffage se produisant dans le réacteur.

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