Nickel carbonyl analyzer

Details Nickel carbonyl analyzer Nickel carbonyl analyzer

G - Physics

01

N

G01N 21/76 (2006.01)

Patent

CA 2525869

Process and apparatus for measuring the concentration of nickel carbonyl in a gaseous nickel carbonyl sample comprising (a) mixing the nickel carbonyl sample with ozone and carbon monoxide under dynamic flow to produce a gaseous mixture with resultant chemiluminescence and photon emission signal; (b) detecting the strength of the signal; and (c) correlating the signal strength with calibrated nickel carbonyl concentration values; the improvement including premixing the ozone and the carbon monoxide to form a pre-mixture prior to mixing with the nickel carbonyl. Most preferably, the signal is measured by an avalanche silicon diode.

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