Oxidation of carbon-boron bonds

Details Oxidation of carbon-boron bonds Oxidation of carbon-boron bonds

C - Chemistry, Metallurgy

07

C

C07C 35/08 (2006.01) C07B 41/02 (2006.01) C07C 29/04 (2006.01) C07C 29/12 (2006.01) C07C 29/48 (2006.01) C07C 33/20 (2006.01) C07C 33/46 (2006.01) C07C 35/28 (2006.01) C07C 35/36 (2006.01) C07D 211/42 (2006.01)

Patent

CA 2351256

Disclosed is a scaleable process for the oxidation of carbon-boron bonds with a monopersulfate compound of the formula 2KHSO5.cndot.KHSO4.cndot.K2SO4. The process may be employed for producing a compound of the formula: (see formula I) from a compound of the formula: (see formula II) (in which R1, R2, R3 and R4 are H, alkyl, etc; and V and W are each H or OH, provided that V and W cannot be both H or both OH), by reacting (II) with a borane and then with the monopersulfate compound. This process provides higher yield and purity than known processes.

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