Photonitrosation of cyclododecane in chloroform in...

Details Photonitrosation of cyclododecane in chloroform in... Photonitrosation of cyclododecane in chloroform in...

C - Chemistry, Metallurgy

07

C

C07C 249/06 (2006.01) C07C 251/44 (2006.01)

Patent

CA 2295956

The invention concerns a method for preparing cyclododecanone oxime which consists in the photochemical reaction of cyclododecanone solubilised in chloroform, a nitrosation agent and hydrogen chloride in a quasi-anhydrous medium, i.e. in conditions such that the reaction medium water content does not exceed 1000 ppm.

L'invention concerne un procédé de préparation d'oxime de la cyclododécanone qui consiste à faire réagir photochimiquement le cyclododécane solubilisé dans le chloroforme, un agent nitrosant et du chlorure d'hydrogène en milieu quasi-anhydre, c'est-à-dire dans des conditions telles que la teneur en eau dans le milieu réactionnel n'excède pas 1000 ppm.

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